Spark ablation device, method for generating nanoparticles by means of said device, and associated uses thereof

Patent details

Status

European patent filed

Application number

EP24382060.2

Priority date

24 January 2024

Inventors

Juan José Vilatela García, Miguel Vázquez Pufleau

Applicant

IMDEA Materials Institute

Transfer opportunity

License of technology

Summary

Spark ablation device used for generating large concentrations (108 particles/cm3) of very small conductive nanoparticles (<5 nm geometric mean size).

Description

Synthesizing nanoparticles in such a way that their concentration and size distribution does not change over time is a challenging task.

Among the different methods for synthesizing nanoparticles, spark discharge is quite promising due to its stability, reliability, and reproducibility. Spark discharge nanoparticle generators (SDGs), also known as spark ablation devices, are based on electrode vaporization by a spark discharge.

Disadvantages of state-of-the-art devices and methods for spark ablation are: (a) their limited nanoparticle production rates due to low spark repetition frequencies (typically in the range of milligrams per hour and with sizes lower than 5 nm up to atomic clusters); (b) emission of large particles formed from dispersions of melted material; and (c) continuous discharge above a certain frequency, stopping particle generation or losing desired particle characteristics. To prevent particles growth, high quenching is necessary, but this is not a very efficient procedure for industrial synthesis.

IMDEA Materials has developed a spark ablation device capable of generating large concentrations (108 particles/cm3) of very small conductive nanoparticles (<5 nm geometric mean size), increasing at least 10-fold the sparking frequency of the SDG as compared to conventional designs.

a) Particle size distribution of the nanoparticles generated with the device of the invention; b) iron nanoparticles size distribution generated with state-of-the-art spark discharge generators.

Contact

Knowledge & Technology Transfer Department, IMDEA Materials Institute

email: techtransfer.materials@imdea.org 

telephone: +34 91 5493422